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超临界流体色谱法测定柴油芳烃含量
引用本文:太史剑瑶,程仲芊,凌凤香.超临界流体色谱法测定柴油芳烃含量[J].当代化工,2014(10):2199-2202.
作者姓名:太史剑瑶  程仲芊  凌凤香
作者单位:中国石化抚顺石油化工研究院,辽宁 抚顺,113001
基金项目:中国石化集团公司资助的石化行业标准修订项目总合-FX1313。
摘    要:采用超临界流体色谱法,测定柴油中单环和多环芳烃的含量。芳烃加标回收实验测定结果的回收率在97.5%~101.6%之间。单环和多环芳烃的重复性实验的测定结果最大偏差不超过0.4个单位。与质谱法分析的数据对比,两种方法的线性相关系数可达到0.99以上。

关 键 词:超临界流体色谱  柴油  芳烃

Determination of Aromatic Content in Diesel Oil by Supercritical Fluid Chromatography
TAI SHI Jian-yao,CHENG Zhong-qian,LING Feng-xiang.Determination of Aromatic Content in Diesel Oil by Supercritical Fluid Chromatography[J].Contemporary Chemical Industry,2014(10):2199-2202.
Authors:TAI SHI Jian-yao  CHENG Zhong-qian  LING Feng-xiang
Affiliation:TAI SHI Jian-yao;CHENG Zhong-qian;LING Feng-xiang;Sinopec Fushun Research Institute of Petroleum and Petrochemicals;
Abstract:Supercritical fluid chromatography was used to determine mono-aromatic and polycyclic aromatic hydrocarbons (PAHs) content of diesel. The experiment of aromatic standard recovery rate showedthat the recovery rate result wasbetween 97.5%-101.6%. The maximum deviation of repeatability experiment for mono-aromatic and polycyclic aromatic hydrocarbons (PAHs) was notmore than 0.4 units. Compared with the method of mass spectrometry, the linear correlation coefficient of the two methods could reach above 0.99.
Keywords:Supercritical fluid chromatography  Diesel  Aromatic hydrocarbon
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