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Decentralised control of chromatographic simulated moving bed processes based on wave front reconstruction
Authors:Tobias Kleinert  Jan Lunze  
Affiliation:aBASF Aktiengesellschaft, Service Center Automation Technology, Carl-Bosch-Straße 38, D-67056 Ludwigshafen, Germany;bRuhr-Universität Bochum, Lehrstuhl für Automatisierungstechnik und Prozessinformatik Universitätsstrasse 150, D-44780 Bochum, Germany
Abstract:The behaviour of chromatographic simulated moving bed processes is described by the movement of concentration profiles through a circle of separation columns. A closed-loop control manipulates the profiles in order to meet demands concerning specified product purity and disturbance attenuation. If steep wave fronts of the concentration profiles occur, the controlled variables undergo fast changes in case of a transient of the process. In this case, a reconstruction of the wave fronts is necessary for a successful control.A simple and effective decentralised controller structure is proposed based on cascaded discrete-time PI controllers. On-line product purity measurements and the reconstructed wave fronts are used for control purposes. Two kinds of process models are used: a rigorous model for dynamic simulations, and strongly simplified plant models for the design of the wave front reconstruction and the controller. The latter models are identified based on experimental step tests with the reference plant and numerical simulations. The performance of the control system is evaluated by numerical simulations.
Keywords:Simulated moving bed  Decentralised control  Wave front reconstruction  State observation  Modelling
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