| 微波消解ICP-MS同时测定色母粒中多种重金属元素 |
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| 引用本文： | 周谙非,杨彦丽. 微波消解ICP-MS同时测定色母粒中多种重金属元素[J]. 食品与发酵工业, 2012, 38(1): 169-171 |
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| 作者姓名： | 周谙非 杨彦丽 |
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| 作者单位： | 国家食品质量安全监督检验中心,北京,100094 |
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| 摘 要： | 采用微波消解-电感耦合等离子体质谱(ICP-MS)法对色母粒中的铅、砷、铜、镉等重金属元素的含量进行了测定,方法快速准确、灵敏度高,加标回收率在96.0%～106.0%,相对标准偏差<3%。
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| 关 键 词： | 微波消解 电感耦合等离子体质谱(ICP-MS) 重金属元素 色母粒 |
Simultaneous Determination of Several Heavy Metal Element in Masterbatch by ICP-MS Microwave Digestion |
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| Zhou An-fei,Yang Yan-li. Simultaneous Determination of Several Heavy Metal Element in Masterbatch by ICP-MS Microwave Digestion[J]. Food and Fermentation Industries, 2012, 38(1): 169-171 |
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| Authors: | Zhou An-fei Yang Yan-li |
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| Affiliation: | (China National Food Quality & Safety Supervision and Inspection Center,Beijing 100094,China) |
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| Abstract: | A method for the simultaneous determination of Pb,As,Cu,Cd in master batch by ICP-MS microwave digestion was studied.This method has simple operation,rapid analysis,highly accurate,reliable,and can be applied in simultaneous determination of heavy metal elements in master batch.Recoveries of the elements from the spiked master batch sample were in the range of 95.2%~101.8%,and the RSD was less than 3%.The results obtained agreed quite well with the certified values. |
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| Keywords: | microwave digestion inductively coupled plasma-mass spectrometry(ICP-MS) heavy metal elements masterbatch |
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