| 精油和芳香萃取物中残留苯含量的测定 |
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| 引用本文： | 闫俊秀,武晓剑. 精油和芳香萃取物中残留苯含量的测定[J]. 香料香精化妆品, 2012, 0(1): 17-20 |
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| 作者姓名： | 闫俊秀 武晓剑 |
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| 作者单位： | 1. 上海应用技术学院,上海,200235
2. 上海香料研究所,上海,200232 |
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| 基金项目： | 上海市科学技术委员会项目 |
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| 摘 要： | 建立了测定精油和芳香萃取物中残留苯含量的方法,分别考察了静态顶空和直接进样两种进样方式、两种不同固定相的色谱柱、氢火焰离子化检测器(FID)和质谱检测器(MSD)两种检测器。实验得出结论:对于挥发性较大的样品采取直接进样的方式进行测定,不易挥发的样品采用顶空进样方式。实验结果表明,在1×10-6～2.5×10-5浓度范围内,采用不同的组合,残留苯含量均具有良好的线性关系。
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| 关 键 词： | 残留苯 精油 芳香萃取物 静态顶空 气相色谱 质谱 |
Determination of Residual Benzene Content in the Essential Oils and Aromatic Extracts |
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| YAN Junxiu , WU Xiaojian. Determination of Residual Benzene Content in the Essential Oils and Aromatic Extracts[J]. Flavour Fragrance Cosmetics, 2012, 0(1): 17-20 |
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| Authors: | YAN Junxiu WU Xiaojian |
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| Affiliation: | 1.Shanghai Institute of Technology,Shanghai 200235,China;2.Shanghai Research Institute of Fragrance ＆ Flavor Industry,Shanghai 200232,China) |
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| Abstract: | A method was developed for the determination of residual benzene content in the essential oils and aromatic extracts.Two injected methods（headspace injection and directed injection）,two different solid-phase columns（HP-5 and HP-1） and two detections（FID and MSD） were discussed.It concludes that the injected method for the more easily volatilized samples is directed injection,and for the less easily volatilized samples is headspace injection.The result shows that the residual benzene content has a good linearity in the concentration between 1×10-6 to 2.5×10-5. |
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| Keywords: | residual benzene essential oils aromatic extracts static-headspace gas chromatography mass spectrum |
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