A first 1,2,4-triazole Pb Complex: Thermal, spectroscopic and structural studies, [Pb2(trz)2(CH3COO)(NO2)]n |
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| Authors: | Ali Akbar Soudi Ali Morsali Sahar Moazzenchi |
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| Affiliation: | aDepartment of Chemistry, Zanjan University, P.O. Box 45195-313, Zanjan, Islamic Republic of Iran;bDepartment of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14115-175, Tehran, Islamic Republic of Iran |
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| Abstract: | A 3D PbII coordination polymer containing 1,2,4-triazole (trz) and two different anions, [Pb2(trz)2(CH3COO)(NO2)]n has been synthesized and characterized by elemental analysis, IR-, 1H NMR-, 13C NMR spectroscopy and studied by thermal as well as X-ray crystallography. The single-crystal X-ray data shows two types of Pb2+-ions with coordination numbers of seven, Pb(1) and Pb(2) with hemidirected and holodirected geometries, respectively. |
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