| 3-(二羟乙基胺基)丙酰胺的合成与表征 |
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| 引用本文： | 贾春贺,刘涛,陈洛亮.3-(二羟乙基胺基)丙酰胺的合成与表征[J].化学推进剂与高分子材料,2010,8(5):52-54. |
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| 作者姓名： | 贾春贺 刘涛 陈洛亮 |
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| 作者单位： | 黎明化工研究院,河南洛阳,471000 |
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| 摘 要： | 以丙烯酰胺和二乙醇胺为原料,通过亲核加成反应合成了一种新型键合剂或中间体3-(二羟乙基胺基)丙酰胺(BEAPAM),探讨了溶剂、原料配比、反应时间的影响,确定了较佳的合成工艺。采用FT-IR、1H-NMR和元素分析等手段对其结构进行表征,结果证明所合成的化合物即为目标化合物。
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| 关 键 词： | 3-(二羟乙基胺基)丙酰胺 合成 表征 推进剂 键合剂 |
Synthesis and Characterization of 3-(bis(2-hydroxyethyl)Amino)Propanamide |
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| JIA Chunhe,LIU Tao,CHEN Luoliang.Synthesis and Characterization of 3-(bis(2-hydroxyethyl)Amino)Propanamide[J].Chemical Propellants & Polymeric Materials,2010,8(5):52-54. |
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| Authors: | JIA Chunhe LIU Tao CHEN Luoliang |
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| Affiliation: | (Liming Research Institute of Chemical Industry,Luoyang 471000,China) |
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| Abstract: | A new bonding agent or intermediate 3-（bis（2-hydroxyethyl） amino） propanamide（BEAPAM） was synthesized with acrylamide and diethanolamine as raw materials by nucleophilic addition reaction.The effects of solvent,raw material proportion and reaction time were discussed.The optimal synthetic process was determined.The structure of obtained product was characterized by FT-IR,1H-NMR and elemental analysis,etc.The results show that the synthesized compound is the objective compound. |
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| Keywords: | 3-（bis（2-hydroxyethyl） amino） propanamide synthesis characterization propellant bonding agent |
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