| 2,6-二氯嘌呤的合成 |
| |
| 引用本文： | 陈文华. 2,6-二氯嘌呤的合成[J]. 化学试剂, 2005, 27(12): 761-762 |
| |
| 作者姓名： | 陈文华 |
| |
| 作者单位： | 常州工程职业技术学院,应用化学系,江苏,常州,213004 |
| |
| 摘 要： | 以氰乙酸甲酯、硫脲为原料,经环合、亚硝化、还原、闭环、硫代、氯化制得标题化合物,6步反应总收率达47.3%.
|
| 关 键 词： | 2 6-二氯嘌呤 氰乙酸甲酯 合成 |
| 文章编号： | 0258-3283（2005）12-0761-02 |
| 收稿时间： | 2005-01-19 |
| 修稿时间： | 2005-01-19 |
Synthesis of 2,6-dichloropurine |
| |
| CHEN Wen-hua. Synthesis of 2,6-dichloropurine[J]. Chemical Reagents, 2005, 27(12): 761-762 |
| |
| Authors: | CHEN Wen-hua |
| |
| Affiliation: | Department of Applied Chemistry, Changzhou Vocation College of Engineering and Technology, Changzhou 213004, China |
| |
| Abstract: | 2, 6-Dichloropufine was synthesized from methyl cyanoacetate and thiourea by cyclization, nitrosation, reduction, eyclization, sulfufization and chloration. The overall yield of the six step reaction was 47.3 %. |
| |
| Keywords: | 2,6- dichloropurine cyanoacetate methyl ester synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
