| 乙酰柠檬酸三丁酯的合成优化 |
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| 引用本文： | 金波,宋同辉,刘尚文. 乙酰柠檬酸三丁酯的合成优化[J]. 广州化工, 2010, 38(11): 105-106,116 |
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| 作者姓名： | 金波 宋同辉 刘尚文 |
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| 作者单位： | 浙江建德建业有机化工有限公司,浙江,建德,311604;浙江建德建业有机化工有限公司,浙江,建德,311604;浙江建德建业有机化工有限公司,浙江,建德,311604 |
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| 摘 要： | 以柠檬酸三丁酯、乙酸酐和正丁醇为原料,采用催化剂TS-121,以共乙酰化—酯化法合成出乙酰柠檬酸三丁酯,并联产乙酸正丁酯。考察了催化剂用量、原料配比、反应温度、反应时间等因素对反应过程的影响,确定了较佳的操作条件。
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| 关 键 词： | 柠檬酸三丁酯 乙酰柠檬酸三丁酯 酯化 乙酰化 |
Synthesis Optimization of Acetyl Tributyl Citrate |
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| JIN Bo,SONG Tong-hui,LIU Shang-wen. Synthesis Optimization of Acetyl Tributyl Citrate[J]. GuangZhou Chemical Industry and Technology, 2010, 38(11): 105-106,116 |
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| Authors: | JIN Bo SONG Tong-hui LIU Shang-wen |
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| Affiliation: | (Zhejiang Jiande Jianye Organic Chemical Co.,Ltd.,Zhejiang Jiande 311604,China) |
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| Abstract: | With tributyl citrate,acetic anhydride and n-butyl alcohol as raw materials,adopting the catalyst TS-121,with total acetyl esterification synthesis method,acetyl tributyl citrate was synthesized and butyl acetate was co-produced.The ratio of raw material,catalyst,reaction temperature and reaction time on the reaction process were studied,and the better operating conditions were determined. |
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| Keywords: | tributyl citrate acetyl tributyl citrate the esterification acetylation |
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