| 1-甲基-4-异丙基-环己-1,2,3,4-四甲酸的合成及光谱分析 |
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| 引用本文： | 林清兰,周文富.1-甲基-4-异丙基-环己-1,2,3,4-四甲酸的合成及光谱分析[J].应用化工,2008,37(10). |
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| 作者姓名： | 林清兰 周文富 |
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| 作者单位： | 三明学院,化学与生物工程系,福建,三明,365004 |
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| 基金项目： | 三明学院大学生创新基金 |
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| 摘 要： | 以松节油和马来酸酐为原料,合成1-甲基-4-异丙基-环己-1,2,3,4-四甲酸的最佳条件为n(萜烯马来酸酐)∶n(KMnO4+H IO4)=0.036∶0.030,pH=0.70,温度80℃,反应2 h,压力101.325 kPa,产率为83%。目标产品用FTIR,UV,XRD,1H NMR测定。
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| 关 键 词： | 1-甲基-4-异丙基-环己-1 2 3 4-四甲酸 合成 结构表征 |
Synthesis and structural analysis of 1-methyl-4-isopropyl-cyclohexyl-1,2,3,4-acid |
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| LIN Qing-lan,ZHOU Wen-fu.Synthesis and structural analysis of 1-methyl-4-isopropyl-cyclohexyl-1,2,3,4-acid[J].Applied chemical industry,2008,37(10). |
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| Authors: | LIN Qing-lan ZHOU Wen-fu |
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| Abstract: | 1-Methyl-4-isopropyl-cyclohexyl-1,2,3,4-acid was synthesized from turpentine and maleic anhydride.The best synthesis conditions were that the mole ratio is n(terpene-maleic anhydride) ∶n(KMnO4+HIO4)=0.036 ∶0.030,the pH is 0.70,the reaction temperature is 80 ℃ and the distillation pressure 101.325 kPa,the yield is 83%,products was characterized by FTIR,UV,XRD,1H NMR. |
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| Keywords: | 1-methyl-4-isopropyl-cyclohexyl-1 2 3 4-acid synthesis characterization |
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