| 亚磷酸二正丁酯的合成 |
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| 引用本文： | 索陇宁. 亚磷酸二正丁酯的合成[J]. 石油化工, 2001, 30(4): 293-295 |
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| 作者姓名： | 索陇宁 |
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| 作者单位： | 兰州石化职业技术学院, |
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| 摘 要： | 研究了用三氯化磷和正丁醇合成亚磷酸二正丁酯的方法 ,讨论了原料配比、反应时间、温度、溶剂用量等因素对反应的影响 ,确定了合成亚磷酸二正丁酯的最佳反应条件 ,在选择的试验条件下产率为 97 1%。
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| 关 键 词： | 亚磷酸二正丁酯 三氯化磷 合成 |
| 文章编号： | 1000-8144(2001)04-0293-03 |
| 修稿时间： | 2000-06-08 |
Synthesis of DibutylPhosphite |
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| SUO Long-ning. Synthesis of DibutylPhosphite[J]. Petrochemical Technology, 2001, 30(4): 293-295 |
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| Authors: | SUO Long-ning |
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| Abstract: | A method for preparing dibutyl phosphite was developed from n - butanol and phosphorus trichloride. The effects of reactant ratio, time, temperature and solvents on the reactions were examined. The optimal reaction conditions were determined. The yield of the product can be up to 97.1％。 |
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| Keywords: | dibutyl phosphite phosphorus trichloride synthesis |
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