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电气石改性聚乳酸切片的制备及分析
引用本文:张琦,于斌,韩建,徐国平,丁新波.电气石改性聚乳酸切片的制备及分析[J].浙江丝绸工学院学报,2012(4):480-483.
作者姓名:张琦  于斌  韩建  徐国平  丁新波
作者单位:[1]浙江理工大学材料与纺织学院‘,杭州310018 [2]浙江理工大学先进纺织材料与制备技术教育部重点实验室,杭州310018
基金项目:浙江省科技厅项目(2011C31011)
摘    要:以聚乳酸母粒为原料,通过添加不同含量的电气石制备聚乳酸改性切片,利用SEM、DSC和毛细管流变仪分别对其表观形貌、热学性能和熔体的流动性能等进行研究。结果表明:改性切片中电气石颗粒的分散较为均匀;结晶度从27%提高到36%,熔点基本不变;随着温度的升高,熔体的表观粘度降低,非牛顿指数增大,并且在同一温度下,流体的表观粘度随着电气石含量的增加呈现先减小后增大的趋势。

关 键 词:聚乳酸  电气石  熔喷非织造布  结晶度  表观粘度

Preparation and Analysis of Polylactic Acid Resin Containing Tourmaline
Authors:ZHANG Qi  YU Bin  HAN Jianb  XU Guo-ping  DING Xin-bo
Affiliation:(Zhejiang Sci-Tech University, a. School of Materials and Textiles; b. The Key Laboratory of Advanced Textile Materials and Manufacturing Technology, Ministry of Education, Hangzhou 310018, China)
Abstract:A modified polylactic acid resin is made by adding different percentage tourmaline prepared, and the surface morphology, thermal properties, rheological behavior are tested by SEM, DSC, and Capil- lary Rheometer, respectively. The results show that the tourmaline exhibite an even distribution in the modified resin. The crystallinity of modified resin raises from 27% to 36%, and the melting point remain unchanged. With the rising of temperature, the apparent viscosity decreases and the non-Newtonian index increases. Besides, at the same temperature, the percentage of tourmaline increases, the apparent viscosity of the fluid decreases firstly and then increases with the increases of the tourmaline content.
Keywords:polylactic acid  tourmaline  meltblowns  crystallinity  apparent viscosity
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