| ZSM—5沸石分子筛的微波辐射法合成与表征 |
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| 引用本文： | 赵杉林 翟玉春. ZSM—5沸石分子筛的微波辐射法合成与表征[J]. 石油学报(石油加工), 1999, 15(3): 89-91 |
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| 作者姓名： | 赵杉林 翟玉春 |
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| 作者单位： | [1]抚顺石油学院应用化学系 [2]东北大学材料与冶金学院 |
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| 摘 要： | 以工业硅溶胶作硅源，用廉价的乙醇作模板剂，用微波辐射的方法合成了ＺＳＭ－５分子筛，探讨了微波晶化时间，微波反应釜压力等合成影响因素，确定了合适的配比范围及合成条件。利用ＸＲＤ，ＳＥＭ等方法对ＺＳＭ－５分子筛的物相和晶貌作了表征。微波辐射法合成的样品粒度小且均匀，并且大大地缩短了反应时间，降低了能耗。
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| 关 键 词： | ZSM－5 分子筛 微波辐射 沸石分子筛 催化剂 合成 |
CHARACTERIZATION AND SYNTHESIS OF ZEOLITE ZSM 5 BY MICROWAVE RADIATION |
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| Zhao Shanlin Zhang Yangjan Sun Guida. CHARACTERIZATION AND SYNTHESIS OF ZEOLITE ZSM 5 BY MICROWAVE RADIATION[J]. Acta Petrolei Sinica (Petroleum Processing Section), 1999, 15(3): 89-91 |
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| Authors: | Zhao Shanlin Zhang Yangjan Sun Guida |
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| Abstract: | The synthesis of zeolite ZSM 5 with alcohol as templating agent by means of microwave radiation was reported.The synthesis conditions of crystallization time and pressure were investigated.The proper feedstock proportion and the technical parameters of preparing molecular sieve ZSM 5 by means of microwave radiation were evaluated.The structure of the crystal and property of the phase were studied by means of XRD and SEM techniques.The crystal size is smaller and more regular than that obtained under the conditions of conventional synthetic method. |
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| Keywords: | ZSM 5 zeolite microwave radiation inorganic synthesis characterization |
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