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Synthesis of iron(Ⅲ)-doped nanostructure TiO2/SiO2 and their photocatalytic activity
Authors:CHEN Rufen  ZHANG Lei  SONG Xiuqin  WEI Yu  HOU Denglu
Abstract:Iron(Ⅲ)-doped nanostructure TiO2-coated SiO2 (TiO2/SiO2) particles were prepared using the layer-by-layer assembly technique and their photocatalytic property was studied. TiO2 colloids were synthesized employing the sol-gel method with TiCl4 as a precursor. The samples were characterized by Fourier transform infrared spectroscopy (FTIR), SEM, EDS, XPS, and XRD. The experimental results show that TiO2 nanopowders on the surface of SiO2 particles are well distributed, the amount of TiO2 is increased with the adding of coating layers, the pure anatase-TiO2 coating layers are synthesized at 500℃, and the photocatalytic activity of Fe3+-doped TiO/SiO2 is higher than tnat of undoped TiO2/SiO2.
Keywords:TiO2 coating  SiO2 particle  nanostructure  layer-by-layer assembly  doping  photocatalytic activity
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