| 微波辅助催化合成己酸异戊酯 |
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| 引用本文： | 钱保华,马卫兴. 微波辅助催化合成己酸异戊酯[J]. 工业催化, 2004, 12(1): 30-31 |
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| 作者姓名： | 钱保华 马卫兴 |
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| 作者单位： | 淮海工学院化学工程系,江苏 连云港 222005 |
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| 基金项目： | 江苏省教育厅自然科学基金资助项目(01KJD150007). |
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| 摘 要： | 报道了以微波辅助由己酸和异戊醇催化合成己酸异戊酯的反应条件。实验结果表明，在醇酸比为1.5、催化剂质量分数为5.1%、辐射功率为420 W和反应时间为20 min时，产率可达90%以上。
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| 关 键 词： | 微波辐射 催化 氯化铁 己酸异戊酯 |
| 文章编号： | 1008-1143(2004)01-0030-02 |
| 修稿时间： | 2003-10-08 |
Catalytic synthesis of isoamyl caproate over ferric chloride with the aid of microwave irradiation |
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| QIAN Bao-hua,MA Wei-xing. Catalytic synthesis of isoamyl caproate over ferric chloride with the aid of microwave irradiation[J]. Industrial Catalysis, 2004, 12(1): 30-31 |
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| Authors: | QIAN Bao-hua MA Wei-xing |
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| Affiliation: | Department of Chemical Engineering , Huaihai Institute of Technology, Jiangsu Lianyungang 222005, China |
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| Abstract: | Synthesis of isoamyl caproate from caproic acid and isoamyl alcohol over ferric chloride with the aid of microwave irradiation was studied. The optimum reaction condition was determined as follows: isoamyl- alcohol-to-caproic-acid molar ratio = 1.5∶1, quantity of the catalyst = 5.1%, irradition power 420 W, reaction time = 20 min. Isoamyl caproate yield of over 90% was obtained under the optimum condition. |
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| Keywords: | microwave irradiation ferric chloride isoamyl caproate mocrowave aided catalysis |
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