| 气质联用法测定纺织品中六溴环十二烷(HBCD) |
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| 引用本文： | 韩欣怡,杨星琦,闫敏,汤晓萍,费沁妮,刘超,陈洁. 气质联用法测定纺织品中六溴环十二烷(HBCD)[J]. 广东化工, 2014, 0(17): 184-185 |
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| 作者姓名： | 韩欣怡 杨星琦 闫敏 汤晓萍 费沁妮 刘超 陈洁 |
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| 作者单位： | 苏州电器科学研究院股份有限公司化学实验室 |
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| 摘 要： | 建立了超声提取纺织品中六溴环十二烷(HBCD)气相色谱/质谱联用仪GC/MS测定含量的分析方法。该方法适用于纺织品中HBCD的检测,HBCD的线性范围为0.5~5.0 mg/L,方法检出限为0.0038 mg/kg,加标回收率为98%~99%,相对标准偏差为1.22%~1.32%。该方法简便可靠,能够达到纺织品中HBCD的检测要求。
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| 关 键 词： | 纺织品 六溴环十二烷 气相色谱/质谱 超声提取 |
Determination of Hexabromocyclododecane in Textiles by GC/MS |
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| Han Xinyi;Yang Xingqi;Yan Min;Tang Xiaoping;Fei Qinni;Liu Chao;Chen Jie. Determination of Hexabromocyclododecane in Textiles by GC/MS[J]. Guangdong Chemical Industry, 2014, 0(17): 184-185 |
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| Authors: | Han Xinyi Yang Xingqi Yan Min Tang Xiaoping Fei Qinni Liu Chao Chen Jie |
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| Affiliation: | Han Xinyi;Yang Xingqi;Yan Min;Tang Xiaoping;Fei Qinni;Liu Chao;Chen Jie;Chemistry Laboratory Suzhou Electrical Apparatus Science Research Institute Stock Co.,Ltd.; |
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| Abstract: | An analytical method was established for the determination of hexabromocyclododecane in textiles with supersonic extraction by gas chromatography-mass spectrometry. With this method to detect HBCD in textiles, the linearity range of HBCD varied from 0.5 mg/L to 5.0 mg/L, the detection limit of this method was 0.0038 mg/kg, the recovery rate were 98 %-99 % with the relative standard deviation 1.22 %-1.32 %. The method was simple and reliable which can meet the requirement of the determination of hexabromocyclododecane in textiles. |
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| Keywords: | textiles： hexabromocyclododecane： GC/MS supersonic extraction |
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