| 水产品中氯霉素残留量气相色谱检测方法的探讨 |
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| 引用本文： | 宫向红,徐英江,张秀珍,刘丽娟. 水产品中氯霉素残留量气相色谱检测方法的探讨[J]. 食品科学, 2006, 27(7): 222-224 |
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| 作者姓名： | 宫向红 徐英江 张秀珍 刘丽娟 |
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| 作者单位： | 山东省海洋水产研究所 |
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| 摘 要： | 本文研究了水产品中氯霉素残留量的气相色谱检测方法,试样用乙酸乙酯提取,蒸干后用0.01mol/L盐酸溶解,正己烷去脂肪,吹干后乙酸乙酯溶解样品,加BSTFA+TMCS(99+1)试剂在超声浴中硅烷化,用气相色谱法测定,外标法定量。当添加水平在0.2～2.0μg/kg时回收率>85%,相对标准偏差为0.9%～2.7%,线性相关系数为0.999。
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| 关 键 词： | 水产品 氯霉素残留 GC |
| 文章编号： | 1002-6630（2006）07-0222-03 |
| 收稿时间： | 2005-08-04 |
| 修稿时间： | 2005-08-04 |
Determination Study on Chloramphenicol Residue in Aquatic Products by Gas Chromatography with Electron Capture Detection (GC-ECD) |
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| GONG Xiang-hong,XU Ying-jiang,ZHANG Xiu-zhen,LIU Li-juan. Determination Study on Chloramphenicol Residue in Aquatic Products by Gas Chromatography with Electron Capture Detection (GC-ECD)[J]. Food Science, 2006, 27(7): 222-224 |
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| Authors: | GONG Xiang-hong XU Ying-jiang ZHANG Xiu-zhen LIU Li-juan |
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| Affiliation: | Shandong Provincial Marine Fisheries Research Institute, Yantai 264003, Chin |
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| Abstract: | The method for determination of chloramphenicol residue in aquatic products by GC-ECD was to be improved. After extraction with ethyl acetate and air evaporation, the residues were dissolved in 0.01mol/L HCl. The lipid was removed with n- hexane to derive the chloramphenicol with BSTFA+TMCS(99+1) in ethyl acetate by a ultrasonic bath. The derivate was determined by GC and quantified by an external standard. The recoveries are above 85% when added with chloramphenicol in a range of 0.2～2.0μg/kg. The relative standard deviations are between 0.9%～2.7%, and the calibration coefficient is 0.999. |
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| Keywords: | GC |
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