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Densification of Nanocrystalline Yttria by Low Temperature Spark Plasma Sintering
Authors:Hidehiro Yoshida  Koji Morita  Byung-Nam Kim  Keijiro Hiraga  Masayasu Kodo  Kohei Soga  Takahisa Yamamoto
Affiliation:National Institute for Materials Science, 1-2-1, Sengen, Tsukuba, Ibaraki, 305-0047, Japan;
Department of Materials Science and Technology, Tokyo University of Science, 2641 Yamazaki, Noda, Chiba, 278-8510, Japan;
Department of Advanced Materials Science, The University of Tokyo, 5-1-5, Kashiwanoha, Kashiwa, Chiba, 277-8561, Japan
Abstract:We investigated the densification of undoped, nanocrystalline yttria (Y2O3) powder by spark plasma sintering (SPS) at sintering temperatures between 650°C and 1050°C at a heating rate of 10°C/min and an applied stress of 83 MPa. In spite of the low sinterability of the undoped Y2O3, a remarkable densification of the powder started at about 600°C, and a theoretical density of more than 97% was achieved at a sintering temperature of 850°C with a grain size of about 500 nm. The low temperature SPS is effective for fabricating dense Y2O3 polycrystals.
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