Densification of Nanocrystalline Yttria by Low Temperature Spark Plasma Sintering |
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Authors: | Hidehiro Yoshida Koji Morita Byung-Nam Kim Keijiro Hiraga Masayasu Kodo Kohei Soga Takahisa Yamamoto |
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Affiliation: | National Institute for Materials Science, 1-2-1, Sengen, Tsukuba, Ibaraki, 305-0047, Japan; Department of Materials Science and Technology, Tokyo University of Science, 2641 Yamazaki, Noda, Chiba, 278-8510, Japan; Department of Advanced Materials Science, The University of Tokyo, 5-1-5, Kashiwanoha, Kashiwa, Chiba, 277-8561, Japan |
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Abstract: | We investigated the densification of undoped, nanocrystalline yttria (Y2O3) powder by spark plasma sintering (SPS) at sintering temperatures between 650°C and 1050°C at a heating rate of 10°C/min and an applied stress of 83 MPa. In spite of the low sinterability of the undoped Y2O3, a remarkable densification of the powder started at about 600°C, and a theoretical density of more than 97% was achieved at a sintering temperature of 850°C with a grain size of about 500 nm. The low temperature SPS is effective for fabricating dense Y2O3 polycrystals. |
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