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Microstructure and properties of in situ nanostructured ceramic matrix composite coating prepared by plasma spraying
Authors:Xueguang Chen  Yong Yang  Dianran Yan  Yanchun Dong  Lei Wang  Jining He  Jianxin Zhang  Xiangzhi Li
Affiliation:(1) Key Laboratory for New Type of Functional Materials in Hebei Province, Hebei University of Technology, Tianjin, China;(2) School of Materials Science and Engineering, Hebei University of Technology, No. 29 Guangrong Road, Hongqiao District, Tianjin, 300132, China;
Abstract:In situ nanostructured ceramic matrix composite coating toughened by metallic phase was fabricated by reactive plasma spraying micro-sized Al–Fe2O3 composite powders. The microstructure of the composite coating was characterized by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy, respectively. The adhesive strength, microhardness, toughness, and wear resistance of the composite coating were explored. The results indicated that the composite coating exhibited dense microstructure with a lot of spherical α-Fe and γ-Al2O3 nano-sized grains embedded within the equiaxed and columnar FeAl2O4 nano-grains matrix. The adhesive strength, toughness, and wear resistance of the composite coating were significantly enhanced despite its lower microhardness compared with the micro-sized Al2O3 coating, which were attributed to the inclusion of ductile metallic phase Fe in the composite coating and the nanostructure of the composite coating.
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