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Studies in the molecular weight distribution of epoxide resins. III. Gel permeation chromatography of epoxide resins subject to postglycidylation
Authors:H. Batzer  S. A. Zahir
Abstract:Unambiguous evidence has been provided for the existence of a branched structure in liquid epoxide resins which have been subjected to postepoxidation with excess epichlorohydrin in the presence of a powerful nucleophilic catalyst, tetramethylammonium chloride. Gel chromatography of the resin on Sephadex LH-20 followed by isolation and identification of the relevant fraction by spectroscopic techniques revealed the presence of a novel trifunctional epoxide having a molecular weight of 680.
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