| (S)-1-叔丁基-2-叔丁氧羰基氨基-天冬氨酸盐半醛的合成 |
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| 引用本文： | 洪伟,王昊.(S)-1-叔丁基-2-叔丁氧羰基氨基-天冬氨酸盐半醛的合成[J].化学试剂,2012,34(3):285-286. |
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| 作者姓名： | 洪伟 王昊 |
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| 作者单位： | 1. 北方民族大学化学与化学工程学院,宁夏银川,750021
2. 宁夏医科大学药学院,宁夏银川,750004 |
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| 摘 要： | 以L-天冬氨酸为原料,经5步反应合成了标题化合物,其结构经比旋光度、1HNMR和13CNMR表征,总收率25%。
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| 关 键 词： | L-天冬氨酸 Swern氧化反应 合成 |
Synthesis of ( S )-1-tert-butyl-2-( tert-butyloxycarbonylamino )-aspartate semi-aldehyde |
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| HONG Wei
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WANG Hao.Synthesis of ( S )-1-tert-butyl-2-( tert-butyloxycarbonylamino )-aspartate semi-aldehyde[J].Chemical Reagents,2012,34(3):285-286. |
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| Authors: | HONG Wei WANG Hao |
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| Affiliation: | 1.School of Chemistry and Chemical Engineering,Beifang University of Nationalities,Yinchuan 750021,China;2.School of Pharmacy,Ningxia Medical University,Yinchuan 750004,China) |
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| Abstract: | (S)-1-tert-Butyl-2-(tert-butyloxycarbonylamino)-aspartate semi-aldehyde was synthesized from L-aspartic acid by a five-step reaction in total yield of 25% and the structure was confirmed by specific rotation,1HNMR and 13CNMR. |
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| Keywords: | L-aspartic acid Swern oxidation reaction synthesis |
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