| S-(2-甲基呋喃-3-基)巯乙酰腙类化合物的合成 |
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| 引用本文： | 周红艳,余爱农,冯驸,胡卫兵.S-(2-甲基呋喃-3-基)巯乙酰腙类化合物的合成[J].化学试剂,2012,34(6):563-564,566. |
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| 作者姓名： | 周红艳 余爱农 冯驸 胡卫兵 |
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| 作者单位： | 湖北民族学院化学与环境工程学院,湖北恩施,445000 |
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| 基金项目： | 湖北省高等学校优秀中青年科技创新团队计划资助项目 |
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| 摘 要： | 以2-甲基-3-呋喃硫醇为原料,经酯化,肼解,得S-(2-甲基呋喃-3-基)巯乙酰肼,再与芳香醛反应,非常方便合成了标题化合物。其结构经IR、1HNMR、MS和元素分析确证。
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| 关 键 词： | 2-甲基-3-呋喃硫醇 乙酰腙 合成 |
Synthesis of S-(2-methylfuran-3-yl) mercapto-acetylhydrazone |
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| ZHOU Hong-yan
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YU Ai-nong
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FENG Fu
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HU Wei-bing.Synthesis of S-(2-methylfuran-3-yl) mercapto-acetylhydrazone[J].Chemical Reagents,2012,34(6):563-564,566. |
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| Authors: | ZHOU Hong-yan YU Ai-nong FENG Fu HU Wei-bing |
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| Affiliation: | *(School of Chemistry and Environmental Engineering,Hubei Institute for Nationalities,Enshi 445000,China) |
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| Abstract: | A series of novel S-(2-methylfuran-3-yl) mercaptoacetylhydrazone have been synthesized by the reaction aromatic aldehydes with S-(2-methylfuran-3-yl) mercaptoacetylhydrazine which was obtained by esterification and hydrazinolysis from 2-methyl-3-furanthiol.The structures were confirmed by IR,1HNMR,MS and elemental analysis. |
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| Keywords: | 2-methyl-3-furanthiol acetylhydrazone synthesis |
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