Preparation and characterization of size controllable spherical silver nanoparticles |
| |
Authors: | Ai-ling Yang Shun-pin Li Yu-jin Wang Xi-chang Bao and Ren-qiang Yang |
| |
Affiliation: | 1. Department of Physics, Ocean University of China, Qingdao, 266100, China 2. Qingdao Institute of Bioenergy & Bioprocess Technology, Chinese Academy of Sciences, Qingdao, 266101, China
|
| |
Abstract: | By adjusting pH values of reactant system, the mass ratio of stabilizer/water and aging temperature, size controllable spherical silver nanoparticles (NPs) were synthesized. The properties of silver NPs are characterized by X-ray diffraction (XRD), transmission electron microscope (TEM) and ultraviolet visible (UV-VIS) absorption spectra. Within the pH values of 7.0–11.0, the aging temperature of 80 °C is better to improve silver NPs in shape to nearly sphere, concentrate size distribution and reduce aggregation than the aging temperature of 25 °C. The shape and dispersibility of silver NPs are the best when the pH of the reactant system is within 7.0–8.0. With pH of 7.5, aging at 80 °C, and stabilizer/water mass ratio of 1%, the spherical silver NPs with sizes of 50–70 nm were synthesized. The results are promising to be used to synthesize core/shell NPs when silver NPs are as core. |
| |
Keywords: | |
本文献已被 CNKI 维普 SpringerLink 等数据库收录! |
| 点击此处可从《光电子快报》浏览原始摘要信息 |
|
点击此处可从《光电子快报》下载全文 |
|