| 三聚氰胺二硝酸盐的合成与表征 |
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| 引用本文： | 张燕,陈雪飞,黄韵东.三聚氰胺二硝酸盐的合成与表征[J].广东化工,2014(7):24+47-24,47. |
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| 作者姓名： | 张燕 陈雪飞 黄韵东 |
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| 作者单位： | 中北大学化工与环境学院,山西太原030051 |
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| 摘 要： | 采用三聚氰胺为原料一步合成目标产物三聚氰胺二硝酸盐(MDN)。利用红外光谱、核磁共振、元素分析等手段对产物的结构进行了表征,反应得率为52.7%。研究了反应温度和反应时间对反应的影响,确定了最佳反应条件为反应时间1h,反应温度95℃。
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| 关 键 词： | 有机化学 含能材料 合成 三聚氰胺 二硝酸盐 |
Synthesis and Characterization of Melaminium Dinitrate |
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| Zhang Yan,Chen Xuefei,Huang Yundong.Synthesis and Characterization of Melaminium Dinitrate[J].Guangdong Chemical Industry,2014(7):24+47-24,47. |
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| Authors: | Zhang Yan Chen Xuefei Huang Yundong |
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| Affiliation: | (Department of Chemistry and Environment, North University of China, Taiyuan 030051, China) |
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| Abstract: | A novel energetic compound melaminium dinitrate （MDN） was synthesized using melamine as starting material. The structure of product were characterized by using infrared spectrum, nuclear magnetic resonance, element analysis, and so on. The yield of this reaction was 52.7 %. The influence of reaction temperature and time on reaction yield was investigated. The optimal reaction conditions were defined as follows： reaction time is lh, reaction temperature is 95 ℃. |
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| Keywords: | organic chemistry synthesis melamine： dinitrate |
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