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纳米Ni-20Fe 颗粒增韧Al2O3复合材料的力学性能与磁性能
引用本文:李合琴,何晓雄,曹闰,秦晓英.纳米Ni-20Fe 颗粒增韧Al2O3复合材料的力学性能与磁性能[J].复合材料学报,2006,23(3):103-107.
作者姓名:李合琴  何晓雄  曹闰  秦晓英
作者单位:1.合肥工业大学材料科学与工程学院, 合肥230009 ;
基金项目:中国科学院"百人计划",安徽省自然科学基金
摘    要:用机械化学及热压烧结方法成功制备了高致密Ni-20Fe/ Al2O3 纳米复合材料。通过X2ray、FE-SEM、力学性能、磁性能测试, 结果表明, 复合后材料断裂韧性从纯α2Al2O3 相的4. 7 MPa·m1/2 提高到6. 2 MPa·m1/2(19 % (Ni-20Fe) / Al2O3 ) , 断裂方式有沿晶断裂和穿晶断裂两种。当Ni-20Fe 合金的体积百分数达到19 %时, 复合材料的饱和磁化强度达33 emu/ g , 矫顽力为200 Oe , 且在低于500 ℃的情况下, 矫顽力基本不随温度而变, 具有良好的磁热稳定性。 

关 键 词:纳米复合材料    氧化铝    Ni-20Fe  合金    饱和磁化强度    机械性能
文章编号:1000-3851(2006)03-0103-05
收稿时间:07 4 2005 12:00AM
修稿时间:2005-07-042005-10-31

Mechanical and magnetic properties of nano-Ni-20Fe tougheningalumina2based nanocomposites
LI Heqin,HE Xiaoxiong,CAO Run,QIN Xiaoying.Mechanical and magnetic properties of nano-Ni-20Fe tougheningalumina2based nanocomposites[J].Acta Materiae Compositae Sinica,2006,23(3):103-107.
Authors:LI Heqin  HE Xiaoxiong  CAO Run  QIN Xiaoying
Affiliation:1.School of Materials Science &|Engineering| Hefei University of Technology| Hefei 230009| China ;2.Institute of Solid State Physics| Chinese Academy of Science| Hefei 230031| China)
Abstract:Ni-20Fe/ Al2O3 nanocomposites with high relative density (D ≥98 %) were fabricated using the mechanochemical method and the hot-pressing process. The fracture toughness is increased f rom 4. 7 to 6. 2 MPa·m1/2 asNi-20Fe volume f raction increases f rom 0 to 19 %. Both the intergranular and the t ransgranular f ractures areobserved on the f racture surface by FE-SEM. When 19 % Ni-20Fe is added , the composite Ms is 33 emu/ g , Hc is200 Oe , and Hc keep s constant below 500 ℃, which shows good magnetic heat stability.
Keywords:nanocomposites  alumina  Ni-20Fe alloy  saturation magnetization  mechanical properties
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