| 气相色谱法测定1,1,3-三甲基-3-苯基茚满 |
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| 引用本文： | 王建刚,王文涛,李健秀,张云涛,郭慧. 气相色谱法测定1,1,3-三甲基-3-苯基茚满[J]. 精细石油化工, 2003, 0(3): 49-50 |
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| 作者姓名： | 王建刚 王文涛 李健秀 张云涛 郭慧 |
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| 作者单位： | 1. 吉林化工学院分析测试中心,吉林,132022
2. 哈尔滨制药总厂研究所,哈尔滨,150000 |
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| 摘 要： | 确立了 1,1,3 三甲基 3 苯基茚满的气相色谱分析法。将试样用甲醇溶解 ,经 5 %SE 30 /ChromosorbW不锈钢色谱柱 (2m× 3mm)分离 ,在柱温为 2 10℃ ,载气 (H2 )流量为 2 0mL/min时 ,在 10min内可完成样品分离 ,平均回收率为 10 1.2 % ,相对标准偏差为 0 .15 %。为 1,1,3 三甲基 3 苯基茚满的质量控制提供了一个简便 ,准确 ,快速的工业分析方法。
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| 关 键 词： | 1,1,3-三甲基-3-苯基茚满 气相色谱 定量分析 |
| 修稿时间： | 2002-10-10 |
DETERMINATION OF 1,1,3-TRIMETHYL-3-PHENYLINDANE BY GAS CHROMATOGRAPHY |
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| Wang Jiangang ,Wang Wentao ,Li Jianxiu ,Zhang Yuntao and Guo Hui. DETERMINATION OF 1,1,3-TRIMETHYL-3-PHENYLINDANE BY GAS CHROMATOGRAPHY[J]. Speciality Petrochemicals, 2003, 0(3): 49-50 |
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| Authors: | Wang Jiangang Wang Wentao Li Jianxiu Zhang Yuntao Guo Hui |
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| Affiliation: | Wang Jiangang 1,Wang Wentao 1,Li Jianxiu 1,Zhang Yuntao 2 and Guo Hui 1 |
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| Abstract: | A method for determination of 1,1,3-trimethyl-3-phenylindane by gas chromatography was developed. The sample was dissolved in methanol, determination of 1,1,3-trimethyl-3-phenylindane could be accomplished in 10 min by 5% Silicone-gum-rubber SE-30/Chromosorb W column at 210 ℃ and the speed of carrier gas (H_2) flow was 20 mL/min.The average recovery was 101.2% and relative standard deviation was 0.15%. Thus it is an easy, quick and accurate method for quality control of 1,1,3-trimethyl-3-phenylindane in industry. |
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| Keywords: | 1 1 3-trimethyl-3-phenylindane gas chromatography quantitative analysis |
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