| 甲乙酮装置尾气中氢气净化吸附剂的工业应用 |
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| 引用本文： | 周广林,周红军,吴全贵.甲乙酮装置尾气中氢气净化吸附剂的工业应用[J].石油炼制与化工,2012,43(2):51-53. |
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| 作者姓名： | 周广林 周红军 吴全贵 |
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| 作者单位： | 中国石油大学（北京）新能源研究中心，北京 102249 |
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| 摘 要： | 开发了用于脱除甲乙酮装置脱氢尾气中的微量甲乙酮和仲丁醇的QMS-01吸附剂，并在工业装置上进行了工业应用。QMS-01吸附剂在脱氢尾气空速90~100 h－1、压力2.4~3.0 MPa、温度5~10 ℃的条件下，可使尾气中甲乙酮质量分数降至小于1 μg/g、仲丁醇质量分数降至小于1 μg/g。工业装置的应用结果表明，QMS-01吸附剂性能稳定，可操作范围宽，可使用3~5年，能满足工业装置的工艺要求。
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| 关 键 词： | 吸附剂 氢气 甲乙酮 仲丁醇 再生 |
| 收稿时间： | 2011-05-27 |
| 修稿时间： | 2011-09-15 |
COMMERCIAL APPLICATION OF ADSORBENT FOR PURIFICATION OF HYDROGEN IN TAIL GAS FROM METHYL ETHYL KETONE UNIT |
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| Zhou Guanglin,Zhou Hongjun,Wu Quangui.COMMERCIAL APPLICATION OF ADSORBENT FOR PURIFICATION OF HYDROGEN IN TAIL GAS FROM METHYL ETHYL KETONE UNIT[J].Petroleum Processing and Petrochemicals,2012,43(2):51-53. |
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| Authors: | Zhou Guanglin Zhou Hongjun Wu Quangui |
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| Affiliation: | (New Energy Research Center,China University of Petroleum,Beijing 102249) |
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| Abstract: | QMS-01 adsorbent for removing methyl ethyl ketone and sec-butyl alcohol from hydrogen were developed and used for the purification of hydrogen in tail gas from methyl ethyl ketone unit.The commercial application results showed that using QMS-01 adsorbent,under appropriate conditions of tail gas space velocity in the range of 90—100 h-1,reaction pressure in the range of 2.4—3.0 MPa and reaction temperature in the range of 5—10 ℃,the mass fraction of methyl ethyl ketone and sec-butyl alcohol in the tail gas could be both less than 1 μg/g.The purified hydrogen could well meet the requirements of hydrogen for hydrogenation processes,and the adsorbent could be regenerated having a service life of about 3—5 years. |
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| Keywords: | adsorbent hydrogen methyl ethyl ketone sec-butyl alcohol regeneration |
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