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快速测定重过磷酸钙中水溶磷和有效磷的超声波法
引用本文:李张胜,赵丽萍.快速测定重过磷酸钙中水溶磷和有效磷的超声波法[J].云南化工,2007,34(2):23-24,28.
作者姓名:李张胜  赵丽萍
作者单位:云南云天化国际化工股份有限公司富瑞分公司,云南,安宁,650309
摘    要:介绍了采用超声波清洗器提取粒状三料重过磷酸钙中的水溶性磷和有效磷的测定方法及提取条件对测定结果的影响,该方法与HG/T 2219~2224-91相比较,具有快速、简便的优点。水溶性磷的测定值与标准方法的绝对偏差<0.3,RSD=0.38%;有效磷的测定值与标准方法的绝对偏差<0.3,RSD=0.26%。

关 键 词:超声波清洗器  提取  水溶性磷  有效磷  重过磷酸钙
文章编号:1004-275X(2007)02-0023-02
修稿时间:2006-12-12

Fast Determination of Water Soluble Phosphorous and Effective Phosphorous from Triple Superphosphate by Ultrasonic Extraction
Li Zhangsheng,Zhao Liping.Fast Determination of Water Soluble Phosphorous and Effective Phosphorous from Triple Superphosphate by Ultrasonic Extraction[J].Yunnan Chemical Technology,2007,34(2):23-24,28.
Authors:Li Zhangsheng  Zhao Liping
Affiliation:Furui Branch, Yunnan Natural Gas Chemical Co. , Ltd. Anning 650309, China
Abstract:Determination of water soluble phosphorous and effective phosphorous by extraction of triple superphosphate with ultrasonic cleaner was introduced, and effect of extraction factors on the result was studied. The method was simpler and quicker than the standard analytical method in HG/T 2219 - 2224 -91, with absolute deviation for the determination of water soluble and effective phosphorous between two methods both lower than 0.3, and the relative standard deviation was respectively less than 0.38% and 0.26%.
Keywords:ultrasonic cleaner  extraction  water soluble phosphorous  effective phosphorous  granular triple superphosphate
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