| 微波法合成MCM-41介孔分子筛及吸附性能研究 |
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| 引用本文： | 孟桂花,王绪根,郭海,吴建宁.微波法合成MCM-41介孔分子筛及吸附性能研究[J].当代化工,2011,40(4):344-346. |
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| 作者姓名： | 孟桂花 王绪根 郭海 吴建宁 |
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| 作者单位： | 1. 石河子大学化学化工学院,新疆石河子,832003
2. 石河子大学化学化工学院,新疆石河子832003;新疆兵团化工绿色过程重点实验室,新疆石河子832003 |
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| 摘 要： | 以十六烷基三甲基氯化铵为模板剂,在微波实验条件下合成MCM-41介孔分子筛,缩短了合成时间,降低产品成本。实验考察了多种因素对MCM-41合成的影响,并通过吸附处理亚甲基蓝溶液能力强弱,得到最佳合成条件：摩尔比1TEOS：0.2CTMACl：160H2O,pH为10,晶化时间15 min。通过红外光谱分析,MCM-41分子筛的主要特征吸收峰均已出现,说明合成分子筛MCM-41成功。
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| 关 键 词： | 介孔分子筛 MCM-41 微波 吸附 |
Microwave Synthesis of MCM-41 Mesoporous Molecular Sieves and Adsorption Research |
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| MENG Gui-hua,WANG Xu-gen,GUO Hai,WU Jian-ning.Microwave Synthesis of MCM-41 Mesoporous Molecular Sieves and Adsorption Research[J].Contemporary Chemical Industry,2011,40(4):344-346. |
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| Authors: | MENG Gui-hua WANG Xu-gen GUO Hai WU Jian-ning |
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| Affiliation: | MENG Gui-hua 1,WANG Xu-gen 1,GUO Hai 1,WU Jian-ning 1,2(1.School of Chemistry and Chemical Engineering,Shihezi University,Xinjiang Shihezi 832003,China,2.Key Laboratory for Green processing of Chemical Engineering of Bingtuan,China) |
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| Abstract: | Using CTMACl as template,mesoporous molecular sieves MCM-41 was synthesized in the microwave experimental conditions,the method can shorten synthesis time and reduce product costs.A variety of factors to affect synthesis of mesoporous molecular sieves MCM-41 were investigated,and through testing the adsorption ability of the gained sieves for methylene blue,the best reaction conditions were gained as follows： TEOS︰CTMACl︰H2O=1︰0.2︰160,pH=10,crystallization time 15 min.Through analysis of IR,main absorption peaks has appeared,which indicates that mesoporous molecular sieves MCM – 41 has successfully been synthesized. |
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| Keywords: | Mesoporous molecular sieves MCM-41 Microwave Adsorption |
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