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间苯二酚法测定淀粉磷酸酯蜜胺盐中氮含量
引用本文:甘春芳,张毅,张雪红. 间苯二酚法测定淀粉磷酸酯蜜胺盐中氮含量[J]. 应用化工, 2010, 39(12)
作者姓名:甘春芳  张毅  张雪红
摘    要:建立了一种快速测定淀粉磷酸酯中氮含量的分析方法,研究了显色剂用量、温度以及络合物稳定性对分析的影响。结果表明,间苯二酚法测定氮含量操作简便,准确度高、精密度好,回收率为92%~105%。含氮量在0~12μg/mL范围内呈线性关系,相关系数为0.999 5,线性关系良好。

关 键 词:淀粉磷酸酯  间苯二酚  氮含量  测定

Determination of nitrogen content in starch phosphate by resorcinol method
GAN Chun-fang,ZHANG Yi,ZHANG Xue-hong. Determination of nitrogen content in starch phosphate by resorcinol method[J]. Applied chemical industry, 2010, 39(12)
Authors:GAN Chun-fang  ZHANG Yi  ZHANG Xue-hong
Abstract:A simple and convenient determination method of nitrogen content in starch phosphate is established.The effects of reagent dosage,temperature and complex stability on analysis were studied.The results showed that the resorcinol method has good precision and accuracy.The determination recovery is 92%~105%,the linear range of the method are 0~12 μg/mL,the coefficient of correlation is 0.999 5.
Keywords:starch phosphate  resorcinol  nitrogen content  determination
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