| 二硫化钼纳米微粒及其单层悬浮液的制备 |
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| 引用本文： | 胡坤宏,胡献国,邵国泉.二硫化钼纳米微粒及其单层悬浮液的制备[J].安徽化工,2007,33(1):38-40. |
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| 作者姓名： | 胡坤宏 胡献国 邵国泉 |
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| 作者单位： | 合肥工业大学机汽学院,安徽,合肥,230009;合肥学院化工系,安徽,合肥,230022;合肥工业大学机汽学院,安徽,合肥,230009;合肥学院化工系,安徽,合肥,230022 |
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| 基金项目： | 合肥学院科研发展研究基金项目（批准号：05ky009zr） |
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| 摘 要： | 利用硫化铵与钼酸钠为原料,制备出非晶态三硫化钼微粒,在氢气氛下煅烧晶化该非晶态三硫化钼,得到30-50nm的片状二硫化钼微粒.将制备的纳米二硫化钼微粒与正丁基锂的正己烷溶液反应48小时,然后将固体产物浸入水中,在超声分散下获得了稳定的纳米二硫化钼悬浮液,最后用XRD、TEM及HRTEM对产物进行了表征.
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| 关 键 词： | 二硫化钼 纳米微粒 单层悬浮液 |
| 文章编号： | 1008-553X（2007）01-0038-03 |
| 收稿时间： | 2006-09-29 |
| 修稿时间： | 2006年9月29日 |
Preparation of Molybdenum Disulfide Nanoparticles and Its Monolayer Suspension |
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| HU Kun-hong,Hu Xian-guo,SHAO Guo-quan.Preparation of Molybdenum Disulfide Nanoparticles and Its Monolayer Suspension[J].Anhui Chemical Industry,2007,33(1):38-40. |
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| Authors: | HU Kun-hong Hu Xian-guo SHAO Guo-quan |
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| Abstract: | Molybdenum trisulfide(MoS3)was first obtained by the fast reaction of ammonium sulfide and sodium molybdate.Molybdenum disulfide nanoparticles with about 30-50 nm sizes were prepared by heating the resultant MoS3 under H2 flow.The intercalation compound of lithium into the so prepared nano-MoS2 was synthesized in the n-butyl lithium solution of n-hexane,and the monolayer nano-MoS2 suspension was obtained by adding water into the resultant intercalation compound.The suspension was characterized by XRD,TEM and HRTEM. |
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| Keywords: | molybdenum disulfide nanoparticles monolayer suspension |
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