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Effect of particle grading on the properties of photosensitive slurry and BaTiO3 piezoelectric ceramic via digital light processing 3D printing
Affiliation:1. State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan 430070, People’s Republic of China;2. School of Materials Science and Engineering, Wuhan University of Technology, Wuhan 430070, People’s Republic of China;3. Advanced Ceramics Institute of Zibo New & High-Tech Industrial Development Zone, Zibo 255000, People’s Republic of China;4. School of Logistics Engineering, Wuhan University of Technology, Wuhan 430070, People’s Republic of China;5. State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430070, People’s Republic of China;1. National Institute for Materials Physics, Atomistilor 405A, Magurele 077125, Romania;2. Polytechnic University of Bucharest, Faculty of Chemical Engineering and Biotechnologies, Department Oxide Materials Science & Engineering, 1-7 Gh. Polizu, Bucharest 011061, Romania;3. National Institute for Lasers, Plasma and Radiation Physics, P.O. Box MG54, 077125 Magurele, Romania;4. Institute of Physical Chemistry “Ilie Murgulescu”, Romanian Academy, 202 Splaiul Independentei, 060021 Bucharest, Romania;5. Dielectrics, Ferroelectrics & Multiferroics Group, Faculty of Physics, Alexandru Ioan Cuza University of Iasi, 700506 Iasi, Romania;1. Wolfson School of Mechanical, Electrical & Manufacturing Engineering, Loughborough University, Loughborough LE11 3TU, United Kingdom;2. Photocentric Limited, Cambridge House, Oxney Road, Peterborough PE1 5YW, United Kingdom;3. Additive Manufacturing Centre of Excellence, 33, Shaftesbury Street South, Derby, DE23 8YH, United Kingdom;1. Electronical Information Materials and Devices Engineering Research Center of Ministry of Education, Guangxi Key Laboratory of Information Materials, and School of Material Science and Engineering, Guilin University of Electronic Technology, Guilin 541004, China;2. School of Material Science and Engineering, Guilin University of Electronic Technology, Guilin 541004, China;3. Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education & International Center for Dielectric Research, School of Electronic Science and Engineering, Xi’an Jiaotong University, Xi’an 710049, PR China;1. School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China;2. Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;3. Space Manufacturing Technology (CAS key Lab), Beijing 100094, China;4. Semiconductor Manufacturing International Corporation, Shanghai 201203, China;1. Department of Biomedical Engineering, University of Southern California, Los Angeles, CA 90089, USA;2. Daniel J. Epstein Department of Industrial and Systems Engineering, University of Southern California, Los Angeles, CA 90089, USA;3. School of Material Science and Engineering, Wuhan University of Technology, Wuhan, Hubei 430070, China;4. Department of Microelectronics, Xidian University, Xi’an, Shanxi 710071, China;5. School of Materials Science and Engineering, Central South University, Changsha, Hunan 410083, China
Abstract:To improve the density and piezoelectric constant of BaTiO3 ceramics prepared by Digital Light Processing 3D printing, the properties of photosensitive slurry were investigated from the perspective of particle grading, and the nitrogen-air two-step debinding and sintering process on the relative density and electrical properties were explored. It was found that as the mass ratio of coarse particles increased, the viscosity, shear stress and cure depth of the slurry decreased. When the mass ratio of fine and coarse particles was 2:8 and sintered at 1350 °C, the ceramic had better performance, with relative density reaching 95.39 ± 0.63 %. The piezoelectric constant d33 was 215 ± 13 pC/N, 29.52 % higher than the single-peak powder. The relative permittivity (εr) and polarization (Pr) were 978 and 16.656 μC/cm2. Finally, BaTiO3 ceramics with Triply Periodic Minimal Surface structures were prepared as piezoelectric sensors, which had the highest output voltage at the same displacement when the mass ratio was 2:8.
Keywords:Digital light processing 3D printing  Barium titanate  Particle grading  Electrical properties  Piezoelectric sensor
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