| 5-氯-2，3-二氢茚-1-酮的合成 |
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| 引用本文： | 龙巧云,李巍,刘东志.5-氯-2，3-二氢茚-1-酮的合成[J].化学工业与工程,2009,26(2):147-149. |
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| 作者姓名： | 龙巧云 李巍 刘东志 |
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| 作者单位： | 天津大学化工学院,天津,300072 |
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| 摘 要： | 对茚虫威关键中间体5-氯-2，3-二氢茚-1-酮的合成进行了研究。以3-氯苄基氯为原料，经亲核取代、水解、脱羧、酰氯化和付氏酰基化等5步反应生成目标产物，产率42％。
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| 关 键 词： | 5-氯-2 3-二氢茚-1-酮 茚虫威 3-氯苄基氯 |
Synthesis of 5-Chloro-2,3-dihydro-1H-inden-1-one |
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| LONG Qiao-yun,LI Wei,LIU Dong-zhi.Synthesis of 5-Chloro-2,3-dihydro-1H-inden-1-one[J].Chemical Industry and Engineering,2009,26(2):147-149. |
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| Authors: | LONG Qiao-yun LI Wei LIU Dong-zhi |
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| Affiliation: | School of Chemical Engineering and Technology;Tianjin University;Tianjin 300072;China |
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| Abstract: | The main intermediate of 5-chloro-2,3-dihydro-1H-inden-1-one in the synthesis of indoxacarb was synthesized in this paper.The title compound was synthesized from 3-chlorobenzyl chloride,through nucleophilic reaction,hydrolyzation,decarboxylation,acyl chloride reaction and Friedel-Crafts acylation reaction in overall yield of 42%. |
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| Keywords: | 5-chloro-2 3-dihydro-1H-inden-1-one indoxacarb 3-chlorobenzyl chloride |
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