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Deformation-induced phase transformation and strain hardening in type 304 austenitic stainless steel
Authors:Amar K De  John G Speer  David K Matlock  David C Murdock  Martin C Mataya  Robert J Comstock Jr
Affiliation:(1) Advanced Steel Processing and Products Research Center, Colorado School of Mines, Golden, CO;(2) Present address: USA Research and Development Center, 3001 E. Columbus Drive, 46312 East Chicago, IN;(3) Advanced Steel Processing and Products Research Center, Department of Metallurgical and Materials Engineering, Colorado School of Mines, 80401 Golden, CO;(4) Advanced Steel Processing and Products Research Center, Department of Metallurgical and Materials Engineering, Colorado School of Mines, 80401 Golden, CO;(5) Micromotion, Division of Emerson, 7070 Winchester Circle, 80301 Boulder, CO;(6) Los Alamos National Laboratory, 87545 Los Alamos, NM;(7) Carbon Steel Product Research, AK Steel Corporation, 45043 Middletown, OH
Abstract:Deformation-induced phase transformation in a type 304 austenitic stainless steel has been studied in tension at room temperature and −50 °C. The evolution of transformation products was monitored using X-ray diffraction (XRD) line profile analysis of diffraction peaks from a single XRD scan employing the direct comparison method. Crystallographic texture transitions due to deformation strain have been evaluated using (111) γ pole figures. The tensile stress-strain data have been analyzed to explain the influence of underlying deformation-induced microstructural changes and associated texture changes in the steel. It is found that the initial stage of rapidly decreasing strain hardening rate in type 304 steel is primarily influenced by hcp ɛ-martensite formation, and the second stage of increasing strain hardening rate is associated with an increase in the α′-martensite formation. The formation of ɛ-martensite is associated with a gradual strengthening of the copper-type texture components up to 15 pct strain and decreasing with further strain at −50 °C. Texture changes during low-temperature deformation not only change the mechanism of ɛ-martensite formation but also influence the strain rate sensitivity of the present steel.
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