Liquid Phase Sintering of Alumina, III. Effect of Trapped Gases in Pores on Densification |
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| Authors: | Weimin Dong Himanshu Jain Martin P Harmer |
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| Affiliation: | Department of Materials Science and Engineering, and the Center for Advanced Materials and Nanotechnology, Lehigh University, Bethlehem, Pennsylvania 18015 |
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| Abstract: | The microstructure evolution and densification kinetics of alumina containing 10 and 20 vol% calcium aluminosilicate glass were studied, for sintering under vacuum and air at 1600°C. Residual porosity was always present in the air-fired samples. The kinetic analysis lent strong support to the notion that trapped gases inhibited the densification and limited the attainment of full density. The samples containing 20 vol% glass were able to reach full density during vacuum sintering. However, the samples containing 10 vol% glass contained some residual porosity even after vacuum sintering, which was attributed to the preferential volatalization of liquid phase. |
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