| 气相色谱法测定神香苏合丸中冰片的含量 |
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| 引用本文： | 张伟,沈亚华.气相色谱法测定神香苏合丸中冰片的含量[J].杭州应用工程技术学院学报,2010(2):85-88. |
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| 作者姓名： | 张伟 沈亚华 |
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| 作者单位： | 杭州胡庆余堂药业有限公司,杭州310016 |
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| 摘 要： | 采用PEG-20M石英毛细管柱，柱温140℃，FID检测器温度280℃，以正十八烷为内标，对神香苏合丸中的冰片进行含量测定。冰片在30～430μg／mL范围内线性关系良好，r=0．9998。平均加样回收率为98．7％（RSD=1．6％）。运用气相色谱法测定神香苏合丸中冰片的含量，方法简便准确、重复性好，可作为神香苏合丸质量控制方法之一。
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| 关 键 词： | 神香苏合丸 冰片 气相色谱法 |
Determination of content of borneol in Shenxiang Suhe pill by GC |
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| ZHANG Wei,SHEN Ya-hua.Determination of content of borneol in Shenxiang Suhe pill by GC[J].Journal of Hangzhou Institute of Applied Engineering,2010(2):85-88. |
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| Authors: | ZHANG Wei SHEN Ya-hua |
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| Affiliation: | (HuqingYutang Pharmaceutical Co. , Ltd. , Hangzhou 310016, China) |
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| Abstract: | The determination was carried out on a PEG-20M capillary column with temperature of 140℃, FID detector with temperature of 280 ℃. The method with internal standard of n-C18 H18 was used to determine the content of borneol in Shenxiang Suhe pill. The borneol sample showed a good linear relationship at the range of 30 ~ 430 μg/mL with r = 0. 999 8. The average recovery was 98.7% with a RSD of 1.6%. The method of gas chromatography applied in the determination of Shenxiang Suhe pill, is simple, accurate, reproducible and can be used for the quality control the Shenxiang Suhe pill. |
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| Keywords: | Shenxiang Suhe pill borneol gas chromatography（GC） |
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