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| 气相色谱法测定大豆中克百威及其代谢物的残留量 | |
| 引用本文： | 谭头云,蔡磊明,贾福艳,王立冬,魏海燕.气相色谱法测定大豆中克百威及其代谢物的残留量[J].农药,2009,48(1). |
| 作者姓名： | 谭头云 蔡磊明 贾福艳 王立冬 魏海燕 |
| 作者单位： | 1. 沈阳化工研究院,沈阳,110021;新疆农业大学,乌鲁木齐,830052 2. 沈阳化工研究院,沈阳,110021 3. 新疆农业大学,乌鲁木齐,830052 |
| 摘 要： | 建立用气相色谱法测定克百威及其代谢物3-羟基克百威在大豆、大豆植株和土壤中残留分析方法。当添加质量分数为0.05～0.2mg/kg时,克百威在大豆、大豆植株和土壤中回收率分别为87.2%～84.8%、87.7%～85.9%、88.6%～87.1%,变异系数在3.6%～5.0%之间;3-羟基克百威在大豆、大豆植株中回收率分别为87.6%～85.2%、89.3%～87.7%,变异系数在1.5%～5.0%之间。 |
| 关 键 词： | 克百威 大豆 气相色谱 残留 |
Determination of Carbofuran and Its Metabolites Residues in Soybean by GC |
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| TAN Tou-yun,CAI Lei-ming,JIA Fu-yan,WANG Li-dong,WEI Hai-yan.Determination of Carbofuran and Its Metabolites Residues in Soybean by GC[J].Pesticides,2009,48(1). | |
| Authors: | TAN Tou-yun CAI Lei-ming JIA Fu-yan WANG Li-dong WEI Hai-yan |
| Abstract: | The residual method of carbofuran and its metabolites 3-hydroxycarbofuran in soybean,the plant of soybean and soil by GC was established.With the addition concentration of 0.05-0.2 mg/kg.The average recovery of carbofuran in soybean,the plant of soybean and soil was 87.2-84.8%,87.7-85.9% and 88.6-87.1%;the coefficient of variation was 3.6-5.0%;and the average recovery of 3-hydroxycarbofuran in soybean and the plant of soybean was 87.6-85.2% and 89.3-87.7%,the coefficient of variation was 1.5-5.0%. |
| Keywords: | carbosulfan soybean gas chromatographic residues |
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