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三甲基烯丙基氯化铵的合成及结构分析
引用本文:尹忠. 三甲基烯丙基氯化铵的合成及结构分析[J]. 化学试剂, 2005, 27(9): 568-570
作者姓名:尹忠
作者单位:西南石油学院,化工院,四川,南充,637001
摘    要:研究了用三甲胺与烯丙基氯为原料合成标题化合物的方法,探索了合成条件,用称量法测定了不同温度、原料配比、反应时间等因素对产率的影响,n三甲胺:n烯丙基氯为1:1.6,55℃通氮气保护条件下反应6h,产率〉90%。对产物的结构进行了分析鉴定。

关 键 词:合成  阳离子单体  季铵盐  三甲基烯丙基氯化铵
文章编号:0258-3283(2005)09-0568-03
收稿时间:2004-10-31
修稿时间:2004-10-31

Synthesis and characterization of trimethylallylammonium chloride
YIN Zhong. Synthesis and characterization of trimethylallylammonium chloride[J]. Chemical Reagents, 2005, 27(9): 568-570
Authors:YIN Zhong
Affiliation:Department of Chemical Engineering, Southwest China Petroleum Institute, Nanchong 637001, China
Abstract:Synthesis of trimethylallylammonium chloride was studied in this paper. Trimethylammonium chloride was allowed to react with allyl chloride under different conditions. The yields at various temperatures , reaction mixture compositions and reaction times were determined. The yields were determined by NaBPh4 gravimetric analysis method. Meanwhile the structure of trimethylallylammomium chloride was characterized by IR and 1^HNMR.
Keywords:synthesis   cationic monomer   quaternary ammonium salt    trimethylallylammonium chloride
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