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In situ observations on the austenite stability in TRIP‐steel during tensile testing
Authors:Suzelotte Kruijver  Lie Zhao  Jilt Sietsma  Erik Offerman  Niels van Dijk  Lawrence Margulies  Erik Lauridsen  Stephan Grigull  Henning Poulsen  Sybrand van der Zwaag
Abstract:In‐situ deformation tests have been performed on a steel displaying the transformation‐induced plasticity (TRIP) effect, while monitoring the phase transformation by means of X‐ray diffraction. A tensile stress is applied to 0.4 mm thick samples of this steel with mass contents of 0.26 % Si, 1.5 % Mn, and 1.8 % Al in a transmission geometry for a synchrotron‐radiation beam of 25 μm · 25 μm. On the diffraction patterns every grain appears as a discrete spot. The austenite {200} reflections are analysed during this investigation. The diffraction patterns are treated like a powder pattern for five different η‐angles, with η representing the angle between the tensile direction and the normal direction of the diffracting {200} planes. The results of the analysis show that η = 0° and η = 90° are the preferential orientations for the transformation to martensite. The Ludwigson and Burger model 9] is used to gain more information about the stress dependence of the deformation induced martensite formation. The microdiffraction patterns also reveal the changes in carbon concentration in austenite at each retained austenite fraction.
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