| 以染料废液为原料合成2-氨基-4-硝基苯酚 |
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| 引用本文： | 王贤丰,刘晓梅,娄桂艳,杨军.以染料废液为原料合成2-氨基-4-硝基苯酚[J].沈阳工业大学学报,1999,21(1):89-91. |
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| 作者姓名： | 王贤丰 刘晓梅 娄桂艳 杨军 |
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| 作者单位： | 1. 沈阳工业大学,沈阳化学工程系,辽宁,沈阳,110023
2. 国家染料工程研究中心,辽宁,沈阳,110021 |
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| 摘 要： | 以分散蓝２ＢＬＮ（Ｃ．Ｉ．分散蓝５６）生产过程中水解工序的废液为原料，经回收得２，４二硝基苯粗 品，然后从硫氢化钠作还原剂，于对７０～７５℃ ， ｐＨ＝７～８条件下将其还原、精制，从而制得高纯度的２～ 氨基－４－硝基苯酚．总收率达６８％，产品纯度≥９８％．
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| 关 键 词： | C I.分散蓝56 水解工序废液 回收 2-氨基-4-硝基苯酚 |
| 修稿时间： | 1997-08-29 |
Synthesis of 2-Amino-4-Nitrophenol From Waste Solution of Dye |
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| Wang Xianfeng,Liu Xiaomei,Lou Guiyan,Yang Jun.Synthesis of 2-Amino-4-Nitrophenol From Waste Solution of Dye[J].Journal of Shenyang University of Technology,1999,21(1):89-91. |
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| Authors: | Wang Xianfeng Liu Xiaomei Lou Guiyan Yang Jun |
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| Affiliation: | Dept. of Chemical Engineering Shenyang Polytechnic University National Research Center of Dye Engineering |
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| Abstract: | 2,4-Dinitrophenol was recoveried from the waste solution of hydrolytic operation sequence produced disperse Blue 2BLN(C.I.Disperse Blue 56), then was partially Reduced with NaHs at 70 ~ 75 and purified with water, formed 2-Amino -4-nitro-phenol. The total yield 68% and purity of product 98%. |
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| Keywords: | C I Disperse Blue 56 waste solution of hydrolytic operation sequence recovery 2-Amino-4-nitrophenol |
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