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MgO部分稳定ZrO2陶瓷制备坩埚的研究
引用本文:陈峥,龙世刚. MgO部分稳定ZrO2陶瓷制备坩埚的研究[J]. 安徽工业大学学报, 2007, 24(2): 130-133
作者姓名:陈峥  龙世刚
作者单位:安徽工业大学,冶金与资源学院,安徽,马鞍山,243002;德国亚琛工业大学,玻璃陶瓷耐火材料研究所
摘    要:以氧化镁(质量分数)为3.5%的Mg-PSZ粉体为原料,向其中添加(质量分数)10%氧化镁悬浊液及化学添加剂,配得氧化镁(质量分数)分别为4.2%和5.8%的氧化镁部分稳定氧化锫材料.以注浆成型法制备感应炉坩埚,考察所制得样品的理化性能.结果表明,在实验所用烧结温度下,与氧化镁质量分数为5.8%相比,氧化镁质量分数为4.2%更有利于四方相生成;同时,延长研磨时间,提高烧结温度和增大样品烧结前后收缩率均有利于增大样品密度,但显气孔率变小,不利于提高样品抗热震性.

关 键 词:钨-铑冶金  氧化镁部分稳定氧化锆  注浆成型
文章编号:1671-7872(2007)02-0130-04
收稿时间:2006-07-12
修稿时间:2006-07-12

Research on Making Crucible by Mg-partially Stabilized Zirconia Ceramic
R.Telle,CHEN Zheng,R.Telle,LONG Shi-gang. Research on Making Crucible by Mg-partially Stabilized Zirconia Ceramic[J]. Journal of Anhui University of Technology, 2007, 24(2): 130-133
Authors:R.Telle  CHEN Zheng  R.Telle  LONG Shi-gang
Abstract:The MgO-partially stabilized zirconia materials whose content is 4.2% and 5.8% MgO are made of 3.5% MgO-partially stabilized zirconia,MgO slurry and chemical additives.Crucible samples are formed by slip casting with that materials.The crucibles's chemical and physical properties were researched.It's found that the phase transformation monoclinic particle to tetragonal of 4.2% Mg-PSZ takes place easily at the experiment sintering temperature.Some factors make Mg-PSZ compacted,such as prolonging milling time,increasing sinter temperature and samples shrinking more,but it makes against thermal shocking of samples while the porosity decreased.
Keywords:W-Rh metallurgy   Mg-partially stabilized zirconia   slip casting
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