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Concentrating Ge in zinc hydrometallurgical process with hot acid leaching-halotrichite method
引用本文:何静,唐谟堂,鲁君乐,刘中清,杨声海,姚维义. Concentrating Ge in zinc hydrometallurgical process with hot acid leaching-halotrichite method[J]. 中南工业大学学报(英文版), 2003, 10(4): 307-312. DOI: 10.1007/s11771-003-0029-3
作者姓名:何静  唐谟堂  鲁君乐  刘中清  杨声海  姚维义
作者单位:School of Metallurgical Science and Engineering,School of Metallurgical Science and Engineering,School of Metallurgical Science and Engineering,Huidong Lead-zinc Mine of Sichuan Province,School of Metallurgical Science and Engineering,School of Metallurgical Science and Engineering Central South University,Changsha 410083,China,Central South University,Changsha 410083,China,Central South University,Changsha 410083,China,Xichang 615205,China,Central South University,Changsha 410083,China,Central South University,Changsha 410083,China
基金项目:Project ( 5 0 2 340 10 )supportedbytheNationalNaturalScienceFoundationofChina
摘    要:1 INTRODUCTIONInthezincconcentratesfromHuidongLead zincMinelocatedinsouth westofChina ,therearerichraremetalssuchasGewhichhasverywideapplica tionsandhighvalue .However ,Gewaslargelywast edbecauseitwasdispersedinalotofresidues(halotrichiteresidue ,Ge Feresidueandhighacidleachedresidue)intheconventionalzinchydrometal lurgicalprocessforthezincconcentrates[1] .InordertoconcentrateandrecoverGe ,anovelhydrometal lurgicalprocess ,ie ,thehotacidleaching halotrichitemethodofzinchasbeendevelope…

收稿时间:2003-03-15
修稿时间:2003-05-15

Concentrating Ge in zinc hydrometallurgical process with hot acid leaching-halotrichite method
He Jing , Tang Mo-tang , Lu Jun-le , Liu Zhong-qing , Yang Sheng-hai and Yao Wei-yi. Concentrating Ge in zinc hydrometallurgical process with hot acid leaching-halotrichite method[J]. Journal of Central South University of Technology, 2003, 10(4): 307-312. DOI: 10.1007/s11771-003-0029-3
Authors:He Jing    Tang Mo-tang    Lu Jun-le    Liu Zhong-qing    Yang Sheng-hai   Yao Wei-yi
Affiliation:(1) School of Metallurgical Science and Engineering, Central South University, 410083 Changsha, China;(2) Huidong Lead-zinc Mine of Sichuan Province, 615205 Xichang, China
Abstract:In recovering Ge and Ag from the calcine and fume dusts mixture of Huidong Lead-zinc Mine, the flow sheet of hot acid leaching-halotrichite method mainly consists of neutral leaching, low-acid leaching, high acid leaching and jarosite precipitation. In the ten circulation periods, the technology flow sheet was carried out smoothly. The loss of Ge in halotrichite residue is less than 5.0%, when iron is precipitated by using ferric potassium alum instead of common Na or ammonium alum and the conditions are controlled at temperature about 95 °C for more than 3 h, pH values below 1. 5. Ge and Ag are concentrated in the high acid leached residue, and their contents are 0.032% and 0.162%, respectively, and the total recovery and direct recovery of zinc are 98.94% and 96.15%, respectively. Foundation item: Project (50234010) supported by the National Natural Science Foundation of China
Keywords:hot-acid leaching  halotrichite process  high-leached residue  Ge
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