| 烧结钽棒提纯工艺研究 |
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| 引用本文： | 李仲香, 张健康, 谢永旭, 陈学清. 烧结钽棒提纯工艺研究[J]. 材料开发与应用, 2023, 38(6): 58-62. |
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| 作者姓名： | 李仲香 张健康 谢永旭 陈学清 |
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| 作者单位： | 1. 宁夏东方钽业股份有限公司, 宁夏 石嘴山 753000;;2. 稀有金属特种材料国家重点实验室, 宁夏 石嘴山 753000;;3. 西北稀有金属材料研究院宁夏有限公司, 宁夏 石嘴山 753000 |
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| 基金项目： | 宁夏回族自治区重点研发计划重点项目（2022BDE92019） |
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| 摘 要： | 对烧结钽棒提纯工艺进行研究，结果表明钽棒等静压成型用包套会造成成型钽棒表面污染，导致碳元素含量增加，钽棒成型选用裂解温度较低的乳胶包套较橡胶包套可以有效降低烧结后钽棒碳元素的残留。高温烧结，能够除去部分残留的杂质，但要完全除尽十分困难。采用HNO3+HF体系酸洗的方式可以有效地去除钽棒表面的夹杂物，达到钽棒提纯的效果。
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| 关 键 词： | 钽棒 成型 烧结 酸洗 |
| 收稿时间： | 2022-06-29 |
Study on Purification Process of Sintered Tantalum Rod |
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| LI Zhongxiang, ZHANG Jiankang, XIE Yongxu, CHEN Xueqing. Study on Purification Process of Sintered Tantalum Rod[J]. Development and Application of Materials, 2023, 38(6): 58-62. |
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| Authors: | LI Zhongxiang ZHANG Jiankang XIE Yongxu CHEN Xueqing |
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| Affiliation: | 1. Ningxia Orient Tantalum Industry Co., Ltd., Shizuishan 753000, China;;2. State Key Laboratory of Special Rare Metal Materials, Shizuishan 753000, China;;3. Northwest Rare Metal Materials Research Institute Ningxia Co., Ltd., Shizuishan 753000, China |
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| Abstract: | The purification process of the sintered tantalum rod is studied, and the results show that sheath for the molding of tantalum rod contributes to the surface contamination, which leads to the increase of C content. The latex sheath with low cracking temperature can effectively reduce the residual C compared with the rubber sheath. High temperature sintering can remove part of the residual impurities, but to completely remove them is very difficult. The HNO3 + HF acid system can effectively remove the inclusion in the surface of the tantalum rod and achieve the purification of the tantalum rod. |
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| Keywords: | tantalum rod molding sintering pickling |
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