| 催化柴油中含氮化合物的研究 |
| |
| 引用本文： | 魏计春,齐邦峰,张会成.催化柴油中含氮化合物的研究[J].化工科技,2010,18(1):60-63. |
| |
| 作者姓名： | 魏计春 齐邦峰 张会成 |
| |
| 作者单位： | 1. 辽宁石油化工大学,研究生学院,辽宁,抚顺,113001;抚顺石油化工研究院,辽宁,抚顺,113001
2. 抚顺石油化工研究院,辽宁,抚顺,113001 |
| |
| 基金项目： | 魏计春（1985-）,男,山东济宁人,辽宁石油化工大学在读硕士研究生,主要从事色谱的研究. |
| |
| 摘 要： | 采用气相色谱-氮化学发光检测器联用技术建立了催化柴油中氮化物类型分布的分析方法,考察了色谱条件对各种氮化物分离的影响,对柴油中60多种氮化物进行了定性、归类。以N,N-二甲基苯胺、4-甲基喹啉、2,4-二甲基喹啉、吲哚、1-甲基吲哚、2,3-二甲基吲哚、2,3,3-三甲基吲哚作为标准样品,考察了各种含氮化合物在氮化学发光检测器上的响应,证实该方法具有很好的重复性和准确度,可用于不同来源和不同加工工艺的柴油馏分中各种氮化物类型及分布的研究。
|
| 关 键 词： | 气相色谱 氮化学发光检测器 氮化物 催化柴油 |
The research of nitrogen compounds in diesel oil |
| |
| WEI Ji-chun,QI Bang-feng,ZHANG Hui-cheng.The research of nitrogen compounds in diesel oil[J].Science & Technology In Chemical Industry,2010,18(1):60-63. |
| |
| Authors: | WEI Ji-chun QI Bang-feng ZHANG Hui-cheng |
| |
| Affiliation: | 1.Graduate School of Liaoning University of Petroleum & Chemical Technology;Fushun 113001;China;2.Fushun Research Institute of Petroleum and Petrochemicals;China |
| |
| Abstract: | The method for the analysis of nitrogen compounds in catalytic diesel oil using gas chromatography-nitrogen chemiluminescence detection(GC-NCD) was established.The effects of chromatogram condition on the resolution time were studied.More than 60 sorts of nitrogen compounds in catalytic diesel oil were determined as well as classified.Take N,N-dimethyaniline,4-methyquinoline,2,4-dimethyquinoline,indole,1-methyindole,2,3-dimethyindole,2,3,3-trimethyindole for standard sample,the responses of nitrogenous comp... |
| |
| Keywords: | Gas chromatography（GC） Nitrogen chemiluminescence detection（NCD ） Nitrogen compounds Diesel oil |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
