Preparation, quality characterization, service performance evaluation and its modification of sapphire crystal for optical window and dome application |
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Authors: | Guigen Wang Hongbo Zuo Huayu Zhang Qibao Wu Mingfu Zhang Xiaodong He Zhaohui Hu Lin Zhu |
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Affiliation: | aShenzhen Graduate School, Harbin Institute of Technology, Shenzhen 518055, PR China;bCenter for Composite Materials, Harbin Institute of Technology, Harbin 150080, PR China;cChina Fangda Group Co. Ltd., Shenzhen 518055, PR China;dShenzhen Taoyuan Middle School, Shenzhen 518055, PR China |
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Abstract: | Sapphire (i.e., Al2O3 single crystal) window and dome are important sensor components. Large-sized sapphire crystal was prepared by an improved Kyropoulos method, and its machining technique of ultrasonic vibration was also reported. The quality and structure were evaluated by illumination of a He–Ne laser transmission electron microscopy (TEM), double crystal X-ray diffraction (DCXRD) and Raman spectroscopy. For practical window and dome application, its high-temperature mechanical strength and optical transmission were both measured, and a modification measure of sputtering Mg film on sapphire surface followed by annealing and subsequent quenching was demonstrated. Large-sized sapphire crystals with high quality and different profiles were successfully grown by adjustment of pulling velocity and crucible size, design of suitable temperature field. Moreover, a series of sapphire windows and domes were fabricated for different optical application. The biaxial flexure strength of sapphire crystal decreases with increasing temperature, and the infrared transmission is also slightly degraded at high temperature. In addition, it should be noted that there is sharp strength drop in the temperature range of 400° to 600 °C which is related with twin formation in sapphire crystal. Submicron MgAl2O4 spinel precipitation can effectively harden sapphire crystal and do not induce large optical-scattering loss, which is a potential modification method for window and dome application of sapphire crystal. |
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Keywords: | Sapphire crystal Window and dome Mechanical-optical properties Precipitation hardening |
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