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海带漂烫水中碘的空气吹出法提取工艺研究
引用本文:张加幸,于跃芹.海带漂烫水中碘的空气吹出法提取工艺研究[J].无机盐工业,2016,48(5):27.
作者姓名:张加幸  于跃芹
作者单位:青岛科技大学化学与分子工程学院,山东青岛 266042
摘    要:采用空气吹出法研究了海带漂烫水中碘的提取工艺,并通过3因素4水平正交实验对体系的pH、温 度、空气通量等工艺条件做了优化,同时探讨了不同氧化剂(NaNO2-H2O2、NaClO和NaNO2)对碘吹出效果的影响。实验得到空气吹出法提取海带漂烫水中碘的最佳工艺条件:pH=2、温度为70 ℃、空气进量为2 L/min,此时碘的最终吹出率可达96.2%。在最佳工艺条件下,分别采用NaNO2-H2O2、NaClO和NaNO2作为氧化剂时,碘的吹出率均可达到90%,表明氧化剂种类对该工艺条件无显著影响。

关 键 词:海带漂烫水    吹出  氧化反应  

Research of iodine extraction process by air blow-out method from kelp blanching waste water
ZHANG Jia-Xing,YU Yue-Qin.Research of iodine extraction process by air blow-out method from kelp blanching waste water[J].Inorganic Chemicals Industry,2016,48(5):27.
Authors:ZHANG Jia-Xing  YU Yue-Qin
Affiliation:College of Chemistry and Molecular Engineering,Qingdao University of Science and Technology,Qingdao 266042,China
Abstract:The air blow-out method was utilized to exact iodine from kelp blanching waste water and the experimental condi- tions,such as pH,temperature,and air flow,were optimized with 3 factors and 4 levels orthogonal tests to improve the iodine exaction rate.In addition,the effects of different oxidizers(NaNO2-H2O2,NaClO,and NaNO2) under the optimized conditions were investigated.Results showed that the optimum reaction conditions were pH of 2.0,temperature of 70 ℃,and air blow-in of 2 L/min.Under the optimized conditions,the exaction rate was up to 96.2%.There is no significant difference on the oxidizing effect among three oxidizers,and the exaction rate all could be up to 90%.Therefore,oxidizing agent′s kind had no obvious effect on the reaction.
Keywords:kelp blanching water  iodine  blow-out  oxidation reaction  
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