| 溶剂法醇解合成3,3,3-三氟丙基三甲氧基硅烷的研究 |
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| 引用本文： | 金小玲,邢建伟,刘必前. 溶剂法醇解合成3,3,3-三氟丙基三甲氧基硅烷的研究[J]. 化工新型材料, 2007, 35(11): 70-72 |
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| 作者姓名： | 金小玲 邢建伟 刘必前 |
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| 作者单位： | 西安工程大学纺织与材料学院,西安,710048;中国科学院化学研究所,北京,100080 |
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| 摘 要： | 以3,3,3-三氟丙基三氯硅烷和甲醇为原料,采用溶剂法醇解合成3,3,3-三氟丙基三甲氧基硅烷,研究了原料配比、N2流量、滴加速度、反应温度及反应时间等因素对合成的影响,运用GC-MS、FT-IR等手段对反应过程和结果进行了综合分析,提出了最佳合成条件.
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| 关 键 词： | 3 3-三氟丙基三甲氧基硅烷 3-三氟丙基三氯硅烷 溶剂法 醇解 |
| 修稿时间： | 2007-06-19 |
Alcoholysis synthesis of 3,3,3-trifluoropropyltrimethoxysilane by solvent method |
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| Jin Xiaoling,Xing Jianwei,Liu Biqian. Alcoholysis synthesis of 3,3,3-trifluoropropyltrimethoxysilane by solvent method[J]. New Chemical Materials, 2007, 35(11): 70-72 |
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| Authors: | Jin Xiaoling Xing Jianwei Liu Biqian |
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| Abstract: | 3,3,3-Trifluoropropyltrimethoxysilane was synthesized by the alcoholysis reaction of 3,3,3-trifluoropropyltrichlorosilane and methanol in an inert solvent.The effects of reaction conditions,such as mole ratio,reaction time,temperature etc.,were studied.The reaction process and composition of products were examined by FT-IR and GC-MS method.The optimum reaction conditions were established. |
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| Keywords: | 3 3 3-trifluoropropyltrimethoxysilane 3 3 3-trifluoropropyltrichlorosilane solvent method alcoholysis |
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