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Preparation and characterization of magnetite/dextran nanocomposite used as a precursor of magnetic fluid
Authors:RY Hong  JH Li  JM Qu  LL Chen  HZ Li
Affiliation:aCollege of Chemistry, Chemical Engineering and Materials Science & Key Laboratory of Organic Synthesis of Jiangsu Province, Soochow University, SIP, Suzhou 215123, China;bState Key Laboratory of Multi-phase Complex Systems, Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100080, China
Abstract:Magnetic nanoparticles were synthesized by the co-precipitation of Fe2+ and Fe3+ using ammonium hydroxide (NH4OH). The obtained nanoparticles were characterized by X-ray powder diffraction, transmission electron microscopy, scanning electron microscopy, Fourier transform infrared (FT-IR) spectroscopy and vibrating sample magnetometer. In order to prepare a biocompatible water-based magnetic fluid, the nanoparticles were modified by dextran through a two-step method. The influences of dextran molecular weight on the size, morphology, coating efficiency and magnetic property of magnetite/dextran nanocomposite were investigated. The magnetite/dextran nanocomposite was dispersed in water to form a magnetic fluid by ball milling. The rheological property of magnetic fluids was investigated using a rotating rheometer.
Keywords:Nanoparticle  Superparamagnetism  Magnetic fluid  Dextran  Rheological property
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