| 相转移催化合成N－取代硫代磷酰胺二乙酯 |
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| 引用本文： | 郭佃顺,黄汝骐,高蓉华,吴志广. 相转移催化合成N－取代硫代磷酰胺二乙酯[J]. 农药, 1995, 0(4) |
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| 作者姓名： | 郭佃顺 黄汝骐 高蓉华 吴志广 |
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| 作者单位： | 山东师范大学化学系 |
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| 摘 要： | 用乙基氯化物（Ｏ，Ｏ－二基硫代磷酰氯）与不同的胺反应，以碱酸钾作缚酸剂、季铵盐作相转移催化剂，合成了六种Ｎ－取代硫代磷酰胺二乙酯，其结构经ＩＲ、ＮＭＲ和元素分析证实。
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| 关 键 词： | N－取代硫代磷酰胺二乙酯，季铵盐，相转移催化，合成 |
Phase Transfer Catalytic Synthesis ofN-Substituted O,O-diethylphosphoramidth-ioates |
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| Guo Dianshun,Huang Ruqi,et al.. Phase Transfer Catalytic Synthesis ofN-Substituted O,O-diethylphosphoramidth-ioates[J]. Pesticides, 1995, 0(4) |
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| Authors: | Guo Dianshun Huang Ruqi et al. |
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| Abstract: | N-Substituted-O,O-diethylphosphoramidothioates(I)were prepared by treating O,O-diethylphos-phorochloridothioate with different amines in the presence ofanhydrous potassium carbonate with quaternary ammoniumsalt as phase transfer catalyst.The cheDlical structures of theproducts were confirmed by elementary analysis,IR and NMRspectra. |
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| Keywords: | N-substituted-O O-diethylphosphoramid-oth-ioate quaternary ammonium salt phase transfer catalysis synthesis |
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