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烧成温度对MgO-TiO2复合无机陶瓷微滤膜支撑体性能的影响
引用本文:许小兵,李旭,杨旭,徐小勇. 烧成温度对MgO-TiO2复合无机陶瓷微滤膜支撑体性能的影响[J]. 无机盐工业, 2022, 54(8): 85-89. DOI: 10.19964/j.issn.1006-4990.2021-0680
作者姓名:许小兵  李旭  杨旭  徐小勇
作者单位:1.巢湖学院化学与材料工程学院,安徽 合肥 2380002.巢湖学院功能材料制备与应用重点实验室
基金项目:安徽高校自然科学研究项目(KJ2019A0686);巢湖学院科研启动基金项目(KYQD-201713);巢湖学院科研项目(XLY-201916)
摘    要:采用添加造孔剂高温烧结法制备了氧化镁-二氧化钛(MgO-TiO2)复合无机陶瓷微滤膜支撑体。分别研究了相同烧结制度下不同最高烧结温度、相同最高烧结温度不同的烧结制度下样品的孔隙率、抗弯强度及纯水通量的变化情况。采用热重分析(TG-DSC)、电子扫描电镜(SEM)和万能试验机等对样品进行热分析、观察样品形貌及抗弯强度等性能测试。研究表明,最高烧结温度和烧结制度对样品的性能有很大影响,采用最高烧结温度为1 400 ℃、升温速率分别为4、8、2 ℃/min的1400-482烧结制度所制备的支撑体的性能最佳,孔隙率为37.57%,抗弯强度为108.65 MPa,纯水通量为4 040 L/(m2?h?MPa)。

关 键 词:MgO-TiO2  烧结制度  陶瓷微滤膜  支撑体  
收稿时间:2021-11-10

Effect of firing temperature on properties of MgO-TiO2 composite inorganic ceramic microfilter membrane support
XU Xiaobing,LI Xu,YANG Xu,XU Xiaoyong. Effect of firing temperature on properties of MgO-TiO2 composite inorganic ceramic microfilter membrane support[J]. Inorganic Chemicals Industry, 2022, 54(8): 85-89. DOI: 10.19964/j.issn.1006-4990.2021-0680
Authors:XU Xiaobing  LI Xu  YANG Xu  XU Xiaoyong
Affiliation:1.College of Material Science and Engineering,Chaohu University,Hefei 238000,China2.Key Laboratory of Functional Material Processing and Application,Chao Hu University
Abstract:MgO-TiO2 composite inorganic ceramic microfilter membrane supports were prepared by adding porous former sintering at high temperature.The changes of porosity,bending strength and pure water flux of the samples under the same sintering system with different maximum sintering temperature and different sintering systems with the same maximum sintering temperature were investigated.Thermal analysis,microstructure and flexural strength of samples were carried out by means of TG-DSC,SEM and strength universal testing machine respectively.Research showed that the maximum sintering temperature and sintering temperature system had great influence on the performance of the samples.The excellent performance of supports with porosity of 37.57%,flexural strength of 108.65 MPa and pure water flux of 4 040 L/(m2?h?MPa) could be fabricated under the maximum sintering temperature of 1 400 ℃ and the sintering temperature system of 1400-482 with the heating rate of 4,8,2 ℃/min.
Keywords:MgO-TiO2  sintering system  ceramic microfiltration membrane  support  
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