| 火焰原子吸收法测定直接氧化锌中的锰 |
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| 引用本文： | 吴道新,张江峰,尹建国.火焰原子吸收法测定直接氧化锌中的锰[J].电工标准与质量,2005,20(2):86-88. |
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| 作者姓名： | 吴道新 张江峰 尹建国 |
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| 作者单位： | [1]长沙理工大学化学与环境工程系，湖南长沙410077／／中南大学化学化工学院，湖南长沙410083 [2]中南大学化学化工学院，湖南长沙410083 |
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| 基金项目： | 湖南省教育厅一般资助项目(04C110) |
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| 摘 要： | 主要研究了在氨性溶液中用Fe(OH)3共沉淀富集直接氧化锌中的痕量锰，分离锌基体后，在5％的硝酸介质中，于原子吸收仪波长279．5m处进行测量．加标回收率在99．0％-104．4％，该法的最大相对标准偏差(RSD)为8．02％．
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| 关 键 词： | 锰直接氧化锌 富集 火焰原子吸收法 |
Determination of Manganese in Zinc Oxide through Flame Atomic Absorption Spectrometry |
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| WU Dao-xian,ZhANG Jiang-feng,YIN Jian-guo.Determination of Manganese in Zinc Oxide through Flame Atomic Absorption Spectrometry[J].Journal of Changsha University of Electric Power(Natural Science Edition),2005,20(2):86-88. |
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| Authors: | WU Dao-xian ZhANG Jiang-feng YIN Jian-guo |
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| Abstract: | An analytical method using iron hydroxide to preconcentrate manganese and to sequentially determine it through flame atomic absorption spectrometry (FAAS) was developed. The preconcentration was treated in ammonium hydroxide solution and zinc ion does not precipitate. The maximum relative standard deviation(R.S.D) was 8.02%,being calculated from eleven measurement. The proposed method may be applied in the determination of manganese in zinc oxide. |
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| Keywords: | manganese direct proceeding zinc oxide preconcentration FAAS |
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